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This indicates that lattice airplanes (0.21 nm) via diamond derive from the brand new graphite (002) jet by lattice distortion. To own area cuatro (FT4), diamond lattice fringes (0.21 nm) get to be the main lattice that have a near disappearance of graphite (002) lattice fringes, appearing one to graphite entirely transits to help you diamond. While in the 150 in order to 210 s, the change inside the Raman spectra is much like that 31 so you can 90 s, guaranteeing the unexpected alter noticed in the surface morphology starts regarding the alternative look of VGs and you can NCD. FESEM images to have trials growing playing with (A) 0 s, (B) 29 s, (C) sixty s, (D) 90 s, (E) 120 s, (F) 150 s, (G) 180 s, and you can (H) 210 s in the second progress process in the step 1,800 W.
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It shows that on the H, O, and you can Ta advanced surroundings of your CVD ecosystem, diamond is created by the stage conversion out of graphite. This also provides an angle to learn the development system of product that have sp2 and sp3 digital setup. X-beam photoelectron spectroscopy (XPS) (Fig. 4A and Si Appendix, Fig. S7) shows obvious Ta and you will O attribute absorption highs, where fresh air atoms try fused having carbon dioxide. Furthermore, HAADF and effort dispersive spectrometry (EDS) mapping photographs (Fig. 4B) reveal atomically distribute Ta atoms. This provides you determination to determine if Ta atoms play a great key part regarding the phase changeover.
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